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Effect of deep cryogenic processing cycles on surface roughness, dimensional stability and microstructure of high carbon high chromium tool steel for cutting tool and dies applications

  • Sachin Lomte

    Mr. Sachin Lomte is working as Associate Professor in the Department of Mechanical Engineering, Maharashtra Institute of Technology, Aurangabad, Maharashtra State, India. He is pursuing his Ph.D. in Mechanical Engineering from Maharashtra Institute of Technology, Aurangabad. He completed his M.E in Mechanical Design and B.E in Production Engineering from Dr. Babasaheb Ambedkar Marathwada University, Aurangabad. He has a total of 20 years of teaching experience. His research interest includes materials science and manufacturing engineering.

    , Ravindra Deshmukh

    Dr. Ravindra Deshmukh is working as Professor in the Department of Mechanical Engineering, Jawaharlal Engineering College Aurangabad, Maharashtra State, India. He completed his Ph.D. in Mechanical Engineering (Manufacturing), M.E in Mechanical Engineering and B.E in Production Engineering from Dr. Babasaheb Ambedkar Marathwada University, Aurangabad. He has a total of 27 years of teaching experience. His research interests include materials science and manufacturing engineering.

    , Tushar Sonar

    Dr. Tushar Sonar is working as a Senior Research Scientist in Department of Welding Engineering, Institution of Engineering and Technology, South Ural State University, Chelyabinsk, Russia. He completed Ph.D. Manufacturing Engineering (Welding) from Annamalai University. He completed his M.Tech. (Mechanical Engineering) from Dr. Babasaheb Ambedkar Marathwada University, Aurangabad, and B.E (Mechanical Engineering) from Pune University. He has a total of 7 years of research work experience. His research interests include welding and joining, additive manufacturing and heat treatment of metals.

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    , Mikhail Ivanov

    Dr. Mikhail Ivanov is working as a Professor and Head of the Department of Welding Engineering, Institution of Engineering and Technology, South Ural State University, Chelyabinsk, Russia. He completed his Ph. D in Technical Science (Foundry) from South Ural State University. He completed his post-graduation in metallurgy from South Ural State University and graduation from South Ural State University. He has total of 17 years of work experience including teaching and research. His research interests include welding and joining, hot tears, cold cracks and simulation of welding phenomena.

    and Visvalingam Balasubramanian

    Dr. Visvalingam Balasubramanian is working as Professor in the Department of Manufacturing Engineering, Annamalai University, Chidambaram, Tamil Nadu State, India. He completed his Ph.D. in Materials Science and Engineering from Indian Institute of Technology Madras (IITM), Chennai. He completed his M. E from College of Engineering Guindy, Anna University, Chennai, and B.E from Government College of Engineering, Salem, University of Madras. He has a total of 28 years of work experience including teaching and research. His areas of interest are Materials Joining, Surface Engineering and Nanomaterials.

Published/Copyright: April 12, 2023
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Abstract

The main objective of this investigation is to analyze the influence of DCT cycles on microstructural evolution, surface roughness, hardness and dimensional stability of AISI D2 tool steel for cutting tools and dies applications. The cryogenic quenching was done using gaseous nitrogen. The AISI D2 tool steel was subjected to two DCT cycle: DCT-I (Hardening + DCT + tempering) and DCT-II (Hardening + tempering + DCT). The dimensional stability of AISI D2 tool steel was evaluated using standard Navy C-ring test. The coordinate measuring machine (CMM) was employed for the precise measurement of Navy C-ring subjected to different DCT cycle. The surface roughness was evaluated with R a (arithmetic mean roughness) and R t (total height of roughness profile) values using surface roughness tester. The microstructural features were analyzed using optical (OM) and scanning electron microscopy (SEM). The electrical resistivity and hardness of treated samples were measured using micro-Ohm meter and Vickers microhardness tester. Results showed that AISI D2 tool steel treated with DCT-I cycle exhibited greater surface finish, hardness and dimensional stability compared to DCT-II cycle. It is mainly attributed to the greater precipitation of finer carbides and balancing of tensile-compressive residual stresses.


Corresponding author: Tushar Sonar, Department of Welding Engineering, Institution of Engineering and Technology, South Ural State University (National Research University), Chelyabinsk, 454080, Russia, E-mail:

About the authors

Sachin Lomte

Mr. Sachin Lomte is working as Associate Professor in the Department of Mechanical Engineering, Maharashtra Institute of Technology, Aurangabad, Maharashtra State, India. He is pursuing his Ph.D. in Mechanical Engineering from Maharashtra Institute of Technology, Aurangabad. He completed his M.E in Mechanical Design and B.E in Production Engineering from Dr. Babasaheb Ambedkar Marathwada University, Aurangabad. He has a total of 20 years of teaching experience. His research interest includes materials science and manufacturing engineering.

Ravindra Deshmukh

Dr. Ravindra Deshmukh is working as Professor in the Department of Mechanical Engineering, Jawaharlal Engineering College Aurangabad, Maharashtra State, India. He completed his Ph.D. in Mechanical Engineering (Manufacturing), M.E in Mechanical Engineering and B.E in Production Engineering from Dr. Babasaheb Ambedkar Marathwada University, Aurangabad. He has a total of 27 years of teaching experience. His research interests include materials science and manufacturing engineering.

Tushar Sonar

Dr. Tushar Sonar is working as a Senior Research Scientist in Department of Welding Engineering, Institution of Engineering and Technology, South Ural State University, Chelyabinsk, Russia. He completed Ph.D. Manufacturing Engineering (Welding) from Annamalai University. He completed his M.Tech. (Mechanical Engineering) from Dr. Babasaheb Ambedkar Marathwada University, Aurangabad, and B.E (Mechanical Engineering) from Pune University. He has a total of 7 years of research work experience. His research interests include welding and joining, additive manufacturing and heat treatment of metals.

Mikhail Ivanov

Dr. Mikhail Ivanov is working as a Professor and Head of the Department of Welding Engineering, Institution of Engineering and Technology, South Ural State University, Chelyabinsk, Russia. He completed his Ph. D in Technical Science (Foundry) from South Ural State University. He completed his post-graduation in metallurgy from South Ural State University and graduation from South Ural State University. He has total of 17 years of work experience including teaching and research. His research interests include welding and joining, hot tears, cold cracks and simulation of welding phenomena.

Visvalingam Balasubramanian

Dr. Visvalingam Balasubramanian is working as Professor in the Department of Manufacturing Engineering, Annamalai University, Chidambaram, Tamil Nadu State, India. He completed his Ph.D. in Materials Science and Engineering from Indian Institute of Technology Madras (IITM), Chennai. He completed his M. E from College of Engineering Guindy, Anna University, Chennai, and B.E from Government College of Engineering, Salem, University of Madras. He has a total of 28 years of work experience including teaching and research. His areas of interest are Materials Joining, Surface Engineering and Nanomaterials.

  1. Author contributions: All the authors have accepted responsibility for the entire content of this submitted manuscript and approved submission.

  2. Research funding: None declared.

  3. Conflict of interest statement: The authors declare no conflicts of interest regarding this article.

References

[1] D. Das, A. K. Dutta, and K. K. Ray, “Correlation of microstructure with wear behaviour of deep cryogenically treated AISI D2 steel,” Wear, vol. 267, nos. 9–10, pp. 1371–1380, 2009, https://doi.org/10.1016/j.wear.2008.12.051.Search in Google Scholar

[2] T. Sonar, S. Lomte, and C. L. Gogte, “Cryogenic treatment of metal–a review,” Mater. Today: Proc., vol. 5, no. 11, pp. 25219–25228, 2018, https://doi.org/10.1016/j.promfg.2018.02.016.Search in Google Scholar

[3] C. H. Surberg, P. Stratton, and K. Lingenhöle, “The effect of some heat treatment parameters on the dimensional stability of AISI D2,” Cryogenics, vol. 48, nos. 1–2, pp. 42–47, 2008, https://doi.org/10.1016/j.cryogenics.2007.10.002.Search in Google Scholar

[4] A. Oppenkowski, S. Weber, and W. Theisen, “Evaluation of factors influencing deep cryogenic treatment that affect the properties of tool steels,” J. Mater. Process. Technol., vol. 210, no. 14, pp. 1949–1955, 2010, https://doi.org/10.1016/j.jmatprotec.2010.07.007.Search in Google Scholar

[5] D. N. Collins, “Classic contributions: cryogenic treatment Deep cryogenic treatment of tool steels: a review,” Int. Heat Treat. Surf. Eng., vol. 2, nos. 3–4, pp. 147–149, 2008, https://doi.org/10.1179/174951508x446367.Search in Google Scholar

[6] D. Das, A. K. Dutta, and K. K. Ray, “Influence of varied cryotreatment on the wear behavior of AISI D2 steel,” wear, vol. 266, nos. 1–2, pp. 297–309, 2010, https://doi.org/10.1016/j.wear.2008.07.001.Search in Google Scholar

[7] K. Moore and D. N. Collins, “Cryogenic treatment of three heat-treated tool steels,” Key Eng. Mater., vol. 86, pp. 47–54, 1993, https://doi.org/10.4028/www.scientific.net/KEM.86-87.47.Search in Google Scholar

[8] M. Pellizzari and A. Molinari, “Deep cryogenic treatment of cold work tool steel,” in Proc. of the 6th Int. Tooling Conf., Karlstad, Sweden, 2002, pp. 547–558.Search in Google Scholar

[9] D. M. Lal, S. Renganarayanan, and A. Kalanidhi, “Cryogenic treatment to augment wear resistance of tool and die steels,” Cryogenics, vol. 41, no. 3, pp. 149–155, 2001, https://doi.org/10.1016/S0011-2275(01)00065-0.Search in Google Scholar

[10] W. T. Cook, “A review of selected steel-related factors controlling distortion in heat-treatable steels,” Heat Treat. Metals, vol. 26, no. 2, pp. 27–36, 1999.Search in Google Scholar

[11] I. S. Jawahir, E. Brinksmeier, R. M’saoubi, et al.., “Surface integrity in material removal processes: recent advances,” CIRP Ann., vol. 60, no. 2, pp. 603–626, 2011. https://doi.org/10.1016/j.cirp.2011.05.002.Search in Google Scholar

[12] D. Das, R. Sarkar, A. K. Dutta, and K. K. Ray, “Influence of sub-zero treatments on fracture toughness of AISI D2 steel,” Mater. Sci. Eng. A, vol. 528, no. 2, pp. 589–603, 2010, https://doi.org/10.1016/j.msea.2010.09.057.Search in Google Scholar

[13] T. Sonar, S. Lomte, C. L. Gogte, and V. Balasubramanian, “Minimization of distortion in heat treated AISI D2 tool steel: mechanism and distortion analysis,” Proc. Manuf., vol. 20, pp. 113–118, 2018, https://doi.org/10.1016/j.promfg.2018.02.016.Search in Google Scholar

[14] R. Thornton, T. Slatter, A. H. Jones, and R. Lewis, “The effects of cryogenic processing on the wear resistance of grey cast iron brake discs,” Wear, vol. 271, nos. 9–10, pp. 2386–2395, 2011, https://doi.org/10.1016/j.wear.2010.12.014.Search in Google Scholar

[15] V. Leskovsek and B. Ule, “Classic contributions: cryogenic treatment Influence of deep cryogenic treatment on microstructure, mechanical properties and dimensional changes of vacuum heat-treated high-speed steel,” Int. Heat Treat. Surf. Eng., vol. 2, nos. 3–4, pp. 155–161, 2008. https://doi.org/10.1179/174951508X446385.Search in Google Scholar

[16] D. Das, A. K. Dutta, and K. K. Ray, “Inconsistent wear behaviour of cryotreated tool steels: role of mode and mechanism,” Mater. Sci. Technol., vol. 25, no. 10, pp. 1249–1257, 2009, https://doi.org/10.1179/174328408X374685.Search in Google Scholar

[17] R. F. Barron, “Cryogenic treatment of metals to improve wear resistance,” Cryogenics, vol. 22, no. 8, pp. 409–413, 1982, https://doi.org/10.1016/0011-2275(82)90085-6.Search in Google Scholar

[18] F. Diekman, Cryogenic Processing: Myths, Methods and Processes, Cincinnati, Ohio, Moldmaking Technology, 1999, pp. 27–31.Search in Google Scholar

[19] J. Patricia, M. Jovičević-Klug, T. Sever, D. Feizpour, and B. Podgornik, “Impact of steel type, composition and heat treatment parameters on effectiveness of deep cryogenic treatment,” J. Mater. Res. Technol., vol. 14, pp. 1007–1020, 2022, https://doi.org/10.1016/j.jmrt.2021.07.022.Search in Google Scholar

[20] R. Schiradely, “Cryogenics-the racers edge,” Heat Treat. Prog., pp. 43–50, 2001.Search in Google Scholar

[21] R. W. Thornton, “Investigating the effects of cryogenic processing on the wear performance and microstructure of engineering materials,” Ph.D. dissertation, University of Sheffield, 2014.Search in Google Scholar

[22] J. D. Darwin, D. M. Lal, and G. Nagarajan, “Optimization of cryogenic treatment to maximize the wear resistance of 18% Cr martensitic stainless steel by Taguchi method,” J. Mater. Process. Technol., vol. 195, nos. 1–3, pp. 241–247, 2008, https://doi.org/10.1016/j.jmatprotec.2007.05.005.Search in Google Scholar

[23] N. B. Dhokey, J. Dandawate, H. Gangurde, and A. Harle, “Metallurgical investigation of cryogenically cracked M35 tool steel,” Eng. Fail. Anal., vol. 21, pp. 52–58, 2012, https://doi.org/10.1016/j.engfailanal.2011.11.013.Search in Google Scholar

[24] N. B. Dhokey, C. Thakur, and P. Ghosh, “Influence of intermediate cryogenic treatment on the microstructural transformation and shift in wear mechanism in AISI D2 steel,” Tribol. Trans., vol. 64, no. 1, pp. 91–100, 2021, https://doi.org/10.1080/10402004.2020.1804652.Search in Google Scholar

[25] A. Bensely, A. Prabhakaran, D. M. Lal, and G. Nagarajan, “Enhancing the wear resistance of case carburized steel (En 353) by cryogenic treatment,” Cryogenics, vol. 45, no. 12, pp. 747–754, 2005. https://doi.org/10.1016/j.cryogenics.2005.10.004.Search in Google Scholar

[26] F. Bouzada, M. Cabeza, P. Merino, and S. Trillo, “Effect of deep cryogenic treatment on the microstructure of an aerospace aluminum alloy,” Adv. Mater. Res., vol. 445, pp. 965–970, 2012, https://doi.org/10.4028/www.scientific.net/AMR.445.965.Search in Google Scholar

[27] C. L. Gogte, A. Likhite, D. Peshwe, A. Bhokarikar, and R. Shetty, “Effect of cryogenic processing on surface roughness of age hardenable AA6061 alloy,” Mater. Manuf. Process., vol. 29, no. 6, pp. 710–714, 2014, https://doi.org/10.1080/10426914.2014.901526.Search in Google Scholar

[28] V. Franco Steier, E. S. Ashiuchi, L. Reißig, and J. A. Araújo, “Effect of a deep cryogenic treatment on wear and microstructure of 6101 aluminum alloy,” Adv. Mater. Sci. Eng., vol. 2016, pp. 1–12, 2016. https://doi.org/10.1155/2016/1582490.Search in Google Scholar

[29] K. M. Asl, A. Tari, and F. Khomamizadeh, “Effect of deep cryogenic treatment on microstructure, creep and wear behaviors of AZ91 magnesium alloy,” Mater. Sci. Eng. A, vol. 523, nos. 1–2, pp. 27–31, 2009, https://doi.org/10.1016/j.msea.2009.06.003.Search in Google Scholar

[30] A. Barylski, K. Aniołek, G. Dercz et al.., “Investigation of micromechanical properties and tribological behavior of WE43 magnesium alloy after deep cryogenic treatment combined with precipitation hardening,” Materials, vol. 14, no. 23, p. 7343, 2021, https://doi.org/10.3390/ma14237343.Search in Google Scholar PubMed PubMed Central

[31] P. Mónica, P. M. Bravo, and D. Cárdenas, “Deep cryogenic treatment of HPDC AZ91 magnesium alloys prior to aging and its influence on alloy microstructure and mechanical properties,” J. Mater. Process. Technol., vol. 239, pp. 297–302, 2017, https://doi.org/10.1016/j.jmatprotec.2016.08.029.Search in Google Scholar

[32] G. E. Totten and S. D. Mackenzie, Handbook of Aluminium – Physical Metallurgy and Processes, New York, USA, Marcel Dekker, 2003, pp. 305–350.Search in Google Scholar

[33] F. Kara and A. Takmaz, “Optimization of cryogenic treatment effects on the surface roughness of cutting tools,” Mater. Test., vol. 61, no. 11, pp. 1101–1104, 2019, https://doi.org/10.3139/120.111427.Search in Google Scholar

[34] L. Singh and J. Singh, “Effect of cryogenic treatment on the microstructure and wear behavior of a T-42 tool steel,” Mater. Test., vol. 57, no. 4, pp. 306–310, 2015, https://doi.org/10.3139/120.110720.Search in Google Scholar

[35] S. Solic, F. Cainer, and V. Leskovsek, “Effect of deep cryogenic treatment on mechanical and tribo-logical properties of PM S390 MC high-speed steel,” Mater. Test., vol. 54, no. 10, pp. 688–693, 2012, https://doi.org/10.3139/120.110380.Search in Google Scholar

[36] P. Raja and R. Malavalamurthi, “Effects of deep cryo treatment of high speed steel on the turning process of a medium carbon steel,” Mater. Test., vol. 59, pp. 763–768, 2017, https://doi.org/10.3139/120.11106910.3139/120.111069.Search in Google Scholar

[37] N. Vasudevan, G. B. Bhaskar, T. Srinivasa Rao, and M. Mohandass, “Mechanical properties of cryogenically treated AA5083 friction stir welds,” Mater. Test., vol. 61, no. 61, pp. 1129–1134, 2019, https://doi.org/10.3139/120.11143010.3139/120.111430.Search in Google Scholar

[38] L. Fang, J. Xiaosong, Z. Yali, S. Hongliang, and S. Zhenyi, “Effect of deep cryogenic treatment on microstructure and mechanical properties of a CoCrFeNiMo medium-entropy alloy,” Mater. Test., vol. 64, no. 4, pp. 463–472, 2022. https://doi.org/10.1515/mt-2021-2049.Search in Google Scholar

[39] T. Sonar, V. Balasubramanian, and S. Malarvizhi, “Mitigation of heat treatment distortion of AA 7075 aluminum alloy by deep cryogenic processing using the Navy C-ring test,” Mater. Test., vol. 63, no. 8, pp. 758–763, 2021, https://doi.org/10.1515/mt-2020-0121.Search in Google Scholar

Received: 2022-12-17
Accepted: 2023-01-24
Published Online: 2023-04-12
Published in Print: 2023-04-25

© 2023 Walter de Gruyter GmbH, Berlin/Boston

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